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Bednarek, P

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Subsequently, the reaction system was diluted with ethyl acetate (200 mL 3), followed by washing with water (100 mL 3) and saturated sodium chloride solution (100 mL 3)

The crude residue was purified by silica gel flash column chromatography ( n -heptane:EtOAc, 2:1) yielding 4-nitrophenyl (2-(pyridin-2-yldisulfaneyl)ethyl) carbonate (89%)