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If you notice the stopper surface deteriorating or if the vial no longer holds vacuum (you don't hear a slight hiss when first puncturing), replace the vial or transfer contents to a fresh sealed container

But they both have meaningful shortcomings that matter if you care about what actually ends up in your research protocol

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10.1016/j.pnpbp.2020.110148 120 van der WesthuyzenJ.Fernandes-CostaF.MetzJ