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Automated high-performance liquid chromatographic method for the determination of guanidinoacetic acid in dried blood spots: a tool for early diagnosis of guanidinoacetate methyltransferase deficiency

These generally show continued safety, but definitive long-term studies don't exist

doi: 10.1016/S0021-9258(17)40528-X 92

The dual HPLC and mass-spec approach is the correct standard, since purity and identity are separate questions and a compound can be pure yet incorrectly identified

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particularly the thyroid-stimulating immunoglobulins subtype)