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Results and Discussion The preparation of the hexapeptide fragment, Fmoc-Asp(OtBu)ValSer(tBu)Ser(tBu)Tyr(tBu)Leu, was accomplished with high efficiency and fidelity via solid-phase peptide synthesis (SPPS) employing the Fmoc/tBu strategy on chlorotrityl chloride (CTC) resin